Least-squares planes (x,y,z in crystal coordinates) and deviations from them (* indicates atom used to define plane) PLANE 1 1.166 (0.047) x + 16.188 (0.031) y - 5.906 (0.087) z = 9.248 (0.051) * 0.000 (0.000) O1 * 0.000 (0.000) O2 * 0.000 (0.000) O3 -0.079 (0.007) Si -1.730 (0.011) O4 2.032 (0.014) N Rms deviation of fitted atoms = 0.000 PLANE 2 2.477 (0.232) x + 0.863 (0.172) y + 17.513 (0.009) z = 5.815 (0.275) Angle to previous plane (with approximate esd) = 73.15 ( 0.66 ) * 0.000 (0.000) O1 * 0.000 (0.000) C1 * 0.000 (0.000) C6 -0.206 (0.046) C7 -0.030 (0.042) Si 0.576 (0.059) N Rms deviation of fitted atoms = 0.000 PLANE 3 8.852 (0.034) x - 8.405 (0.099) y - 3.804 (0.389) z = 7.154 (0.095) Angle to previous plane (with approximate esd) = 75.14 ( 1.79 ) * 0.000 (0.000) O2 * 0.000 (0.000) C9 * 0.000 (0.000) C14 -0.014 (0.042) C8 -0.130 (0.040) Si -0.892 (0.053) N Rms deviation of fitted atoms = 0.000 PLANE 4 7.471 (0.174) x + 7.156 (0.272) y + 6.190 (0.282) z = 10.068 (0.192) Angle to previous plane (with approximate esd) = 64.62 ( 1.32 ) * 0.000 (0.000) O3 * 0.000 (0.000) C16 * 0.000 (0.000) C21 -0.148 (0.049) C15 -0.042 (0.045) Si 0.591 (0.062) N Rms deviation of fitted atoms = 0.000 ************************************************************************ Selected torsion angles (and their esd) O2 - Si - O1 - C1 67.21(1.42) O3 - Si - O1 - C1 -103.33(1.34) O4 - Si - O1 - C1 163.32(1.26) N - Si - O1 - C1 -17.81(1.27) O1 - Si - O2 - C14 -100.53(1.44) O3 - Si - O2 - C14 69.95(1.61) O4 - Si - O2 - C14 163.17(1.43) N - Si - O2 - C14 -15.78(1.44) O1 - Si - O3 - C21 66.00(1.46) O2 - Si - O3 - C21 -104.50(1.37) O4 - Si - O3 - C21 160.92(1.33) N - Si - O3 - C21 -19.00(1.34) O1 - Si - O4 - C28 -63.30(1.10) O2 - Si - O4 - C28 56.79(1.11) O3 - Si - O4 - C28 177.03(1.08) O1 - Si - N - C15 -74.05(0.86) O2 - Si - N - C15 165.99(0.88) O3 - Si - N - C15 45.70(0.87) O1 - Si - N - C7 45.65(0.87) O2 - Si - N - C7 -74.31(0.89) O3 - Si - N - C7 165.39(0.89) O1 - Si - N - C8 166.32(0.87) O2 - Si - N - C8 46.35(0.86) O3 - Si - N - C8 -73.94(0.84) Si - O1 - C1 - C2 178.43(1.00) Si - O1 - C1 - C6 1.56(2.18)